A pressure‐ and temperature‐controlled sample cell for the structural investigation of lyotropic liquid crystals using a small‐angle x‐ray diffraction line source
作者:
P. M. Duesing,
R. H. Templer,
J. M. Seddon,
期刊:
Review of Scientific Instruments
(AIP Available online 1996)
卷期:
Volume 67,
issue 12
页码: 4228-4234
ISSN:0034-6748
年代: 1996
DOI:10.1063/1.1147573
出版商: AIP
数据来源: AIP
摘要:
We present the design and performance of a temperature‐ and pressure‐controlled sample cell for the small‐angle x‐ray diffraction analysis of lyotropic liquid crystalline materials. The particular requirements for such a system of high resolution, high intensity, and control on sample homogeneity can be particularly well fulfilled using line‐source diffraction. We thus designed a sample cell that will allow the use of a line source. Sample volume is kept small (20 &mgr;l) to keep the contained energy low. The hydrostatic system, based on beryllium x‐ray windows, Bridgman type seals with lead O rings and a stainless‐steel body is rated to achieve pressure control within ±3 bar between 0 and 3000 bar at ramping rates of 30–100 bar/s. Temperature control is achieved within ±0.03 K between room temperature and 180 °C. Maximum heating rates correspond to 0.8 K/s. Control algorithms are implemented on a Microrobotics K4 controller, using a modest amount of computing power. ©1996 American Institute of Physics.
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