2D NMR Studies of Octahydroindole Svstems
作者:
IgnacioH. Sanchez,
MariaIsabel Larraza,
Irma Rojas,
Francisco Kuri,
Eduardo Diaz,
André Aumelas,
Krzysztof Jankowski,
期刊:
Spectroscopy Letters
(Taylor Available online 1987)
卷期:
Volume 20,
issue 2
页码: 125-147
ISSN:0038-7010
年代: 1987
DOI:10.1080/00387018708081534
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
The1H and13C NMR resonances of title compounds were assigned by using 2D and decoupling techniques. The stereochemistry of ring fusion was identified by using, in particular, NOE and COSY1H1H experiments. The low temperature COSY enables the evaluation of the relative populations (2:1) of N-acyl forms of isomeric octahydroindoles resolvable at −60°C.
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