Cross-sectional transmission electron microscopy of electrodeposited Ni-P alloys
作者:
ByK. Shimizu,
G.E. Thompson,
G.C. Wood,
K.K. Kobayashi,
期刊:
Philosophical Magazine Letters
(Taylor Available online 1990)
卷期:
Volume 61,
issue 2
页码: 43-48
ISSN:0950-0839
年代: 1990
DOI:10.1080/09500839008206478
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
Ultramicrotoming has been employed to prepare thin cross-sections of Ni-P alloys electrodeposited on to a copper substrate. The sections, as thin as 10nm or even less, can be prepared readily with negligible damage to the alloys. Subsequent examination of the ultramicrotomed sections in an analytical transmission electron microscope has revealed that Ni-P alloys of low P content consist of fine layers of different composition and crystallinity. High-resolution transmission electron microscopy of ultramicrotomed sections has also revealed the presence of ordered regions, a few nanometres in size, in the Ni77P23alloy which has been thought previously to be amorphous.
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