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Technique for Preparing Laminated Pole Figure Samples

 

作者: Sam Leber,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1965)
卷期: Volume 36, issue 12  

页码: 1747-1750

 

ISSN:0034-6748

 

年代: 1965

 

DOI:10.1063/1.1719455

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A new method is described for making composite samples for the x‐ray diffraction, back reflection pole figure technique. Considerable savings, in material and machining costs, are realized by cutting strips, for lamination, at 45° to the rolling direction. The required reference surface is obtained, during lamination, by maintaining an angle of 54.7° between the strips and the surface developed by the cut edges. The advantages of the composite technique (better averaging, minimization of errors, and evaluation of random intensity from the pole figure data) are retained by this modification.

 

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