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The Crystal and Molecular Structure of 4-Pentylphenyl-4′-Pentioxythiobenzoate (5S5)

 

作者: J. Chruściel,   B. Pniewska,   M.D. Ossowska-Chruściel,  

 

期刊: Molecular Crystals and Liquid Crystals Science and Technology. Section A. Molecular Crystals and Liquid Crystals  （Taylor Available online 1995）
卷期: Volume 258, issue 1  

页码: 325-331

 

ISSN:1058-725X

 

年代: 1995

 

DOI:10.1080/10587259508034572

 

出版商: Taylor & Francis Group

 

关键词: Liquid crystal;crystal and molecular structure.

 

数据来源: Taylor

 

摘要:

The 4-pentylphenyl-4′-pentoxythiobenzoate (5S5), C23H30O2S, crystallizes in the monoclinic system: space group P21/c, a = 19.817 (2) Å, b = 5.585 (1) Å, c = 20.238 (2) Å,β∼ 104.792 (8)°, z = 4. The structure was solved by direct methods and refined to the final R = 0.065, for 3415 observed reflections. The pentoxythiobezoate moiety is nearly planer. Molecular rows form an interclated structure. C‒H…O type short intermolecular contacts were found.

 

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