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An improved lamellae drop-off technique for sharp tip preparation in scanning tunneling microscopy

 

作者: M. Klein,   G. Schwitzgebel,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1997)
卷期: Volume 68, issue 8  

页码: 3099-3103

 

ISSN:0034-6748

 

年代: 1997

 

DOI:10.1063/1.1148249

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A superior lamellae etching drop-off technique is described for the preparation ofWtips without the use ofCCl4.Sharp tips with an apex of 25 nm or less can be produced routinely. In the case of Pt/Ir wire, the chemical inertness of the material means that it has to be reduced in diameter before being etched to yield a tip. In order to accomplish this, a capillary diameter reduction technique has also been developed for use in combination with the lamellae etching drop-off technique. The apparatus does not require the use of micromanipulators or micromovers. The shapes of tips with apexes as small as 25 nm can be investigated by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). This low cost method of producing sharp tips scanning tunneling microscopy is very effective and it would probably be feasible to develop an automatic tip preparation with a little more technical effort. Since it is possible to produce well shapedWtips almost every time after acquiring a little skill, it is not usually necessary to check their shape by TEM or SEM before use. In contrast, the success rate with Pt/Ir tips is only up to 70&percent;, so that it is advisable to check their shapes by TEM. ©1997 American Institute of Physics.

 

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