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Low magnetic field dynamic nuclear polarization using a single-coil two-channel probe

 

作者: Dinh M. TonThat,   Matthew P. Augustine,   Alexander Pines,   John Clarke,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1997)
卷期: Volume 68, issue 3  

页码: 1527-1531

 

ISSN:0034-6748

 

年代: 1997

 

DOI:10.1063/1.1147641

 

出版商: AIP

 

数据来源: AIP

 

摘要:

We describe the design and construction of a single-coil, two-channel probe for the detection of low-field magnetic resonance using dynamic nuclear polarization (DNP). The high-frequency channel of the probe, which is used to saturate the electron spins, is tuned to the electron Larmor frequency, 75 MHz at 2.7 mT, and matched to 50 &OHgr;. Low-field,1H nuclear magnetic resonance (NMR) is detected through the second, low-frequency channel at frequencies <1 MHz. The performance of the probe was tested by measuring the DNP of protons in a manganese (II) chloride solution at 2.7 mT. At the proton NMR frequency of 120 kHz, the signal amplitude was enhanced over the value without DNP by a factor of about 200. ©1997 American Institute of Physics.

 

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