Simultaneous Determination of Dipropyl Pyridine-2,5-Dicarboxylate, N-Octyl Bicycloheptene Dicarboximide, Piperonyl Butoxide, and Pyrethrins in Pet Shampoo by Reversed Phase High Performance Liquid Chromatography
作者:
I.-H. Wang,
R. Moorman,
J. Burleson,
期刊:
Journal of Liquid Chromatography & Related Technologies
(Taylor Available online 1996)
卷期:
Volume 19,
issue 20
页码: 3293-3304
ISSN:1082-6076
年代: 1996
DOI:10.1080/10826079608014580
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
A reverse phase high performance liquid chromatographic method has been developed for the simultaneous determination of six pyrethrin esters, piperonyl butoxide (PBO), dipropyl pyridine-2,5-dicarboxylate (MGK 326), and endo- and exo-N-octyl bicycloheptene dicarboximide (MGK 264) in pet shampoo formulations. A C8Octyl reverse phase column and different compositions of acetonitrile, methanol and water as mobile phases were used. The eluent was monitored with UV absorption at 220, 230, 240 and 225 nm. Internal standard calculations using peak area was used to calculate each active ingredient peak. Interfering inert ingredients were separated from all active ingredients using this method. This simple and reliable technique has an advantage over GC because of the thermal degradation of pyrethrins, and over normal phase high performance liquid chromatography, since it requires no further sample clean-up.
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