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Increased precision in strain measurement of diamond by microRaman spectroscopy

 

作者: W. Brock Alexander,   Paul H. Holloway,   Joseph Simmons,   Romulo Ochoa,  

 

期刊: Journal of Vacuum Science&Technology A: Vacuum, Surfaces, and Films  (AIP Available online 1994)
卷期: Volume 12, issue 5  

页码: 2943-2945

 

ISSN:0734-2101

 

年代: 1994

 

DOI:10.1116/1.578973

 

出版商: American Vacuum Society

 

关键词: DIAMONDS;THIN FILMS;SPUTTERED MATERIALS;TUNGSTEN;INTERNAL STRAINS;MEASURING METHODS;RAMAN SPECTRA;CALIBRATION;ACCURACY;diamonds;W

 

数据来源: AIP

 

摘要:

MicroRaman spectroscopy has been used to measure stress in diamond with improved precision. Stress was induced by rf sputter deposited tungsten films of 1‐ and 9‐μm thickness. Preliminary data showed a systematic error in the diamond Raman peak position of about 0.05 cm−1/scan, which led to inaccurate and imprecise stress measurement. A new technique, using a reference 5520‐Å krypton line only 10.5 cm−1from the Raman diamond line, results in an order of magnitude increase in measurement precision. Using this calibration, diamond peak position could be measured with a precision of ±0.03 cm−1which corresponds to ±11 MPa of stress. This is an easy and inexpensive means to improve stress measurements in diamond by microRaman spectroscopy.

 

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