A Facile Synthesis of Aldehyde and Ketone via Senochemical Barbier Reaction and Oxidation
作者:
Adam Shih‐Yuan Lee,
Chih‐Chun Kung,
期刊:
Journal of the Chinese Chemical Society
(WILEY Available online 1997)
卷期:
Volume 44,
issue 1
页码: 65-69
ISSN:0009-4536
年代: 1997
DOI:10.1002/jccs.199700010
出版商: WILEY‐VCH Verlag
关键词: Sonochemical;Barbier reaction;Oxidation;Methyl ketone;Ultrasound
数据来源: WILEY
摘要:
AbstractMethyl ketone is prepared by a sonochemical Barbier reaction of methyl iodide, magnesium powder and aldehyde in Benzene/THF (9/1) solvent in a commercial ultrasonic cleaning bath (39 kHz), followed by the addition of N‐chlorosuccinimide (NCS) as an oxidizing agen
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