The Use of Silar 10 CP for the Packed Column Gas Chromatographic Determination of Chlorophenoxyacetic Acid Herbicides in Water and Sediments
作者:
S.M. Waliszewski,
V.T. Pardio Sedas,
期刊:
International Journal of Environmental Analytical Chemistry
(Taylor Available online 1992)
卷期:
Volume 49,
issue 4
页码: 231-238
ISSN:0306-7319
年代: 1992
DOI:10.1080/03067319208027574
出版商: Taylor & Francis Group
关键词: Chlorophenoxyacetic acid;water;sediments;GC-ECD
数据来源: Taylor
摘要:
The determination of chlorophenoxyacetic acid herbicide residues was done with GC-ECD as pentafluorobenzyl derivatives. The herbicides were separated on a 3% Silar 10 CP column, which permits better resolution from interfering organic acids of environmental origin. The fortification study provides an 84–91% recovery for the water and sediment samples. The detection limits were established as 0.1 μg/1 for the water and 1.0–1.5 ng/g for the sediment samples. The use of a 3%Silar 10 CP packed column in the monitoring study as compared with a 1.5% OV-17 + 1.95% QF-1 one, shows the very small amount of contamination of the samples with these herbicide classes.
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