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High Performance Liquid Chromatography and Electron Spin Resonance Studies of Some Sugar-Nitroxide Solutions

 

作者: J.P. Agnel,   C. Thiéry,   C. Battesti,   P. Vincent,   J. Raffi,  

 

期刊: Analytical Letters  （Taylor Available online 1985）
卷期: Volume 18, issue 8  

页码: 1013-1025

 

ISSN:0003-2719

 

年代: 1985

 

DOI:10.1080/00032718508066196

 

出版商: Taylor & Francis Group

 

关键词: EBR;spin-trapping;nitroxide;sugar;HPLC.

 

数据来源: Taylor

 

摘要:

Radicals induced by gamma irradiation of alpha-D-glucose, 1-0-methyl-alpha-D-glucose and maltose, in the solid state, have been studied by the spin-trapping method. High performance liquid chromatography of sugar-nitroxide solutions, combined with electron spin resonance analysis, revealed nine, eight and twelve discernible radical species, the majority of them being indiscernible by the direct spin-trapping method. Tentative correlations and assignments of chemical structures are discussed.

 

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