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1-Propenyl 4,6-Q-Benzylidene-β-D-Mannopyranoside-2,3-Cyclic Sulfate: A Substrate for the Synthesis of [F-18] 2-Deoxy-2-Fluoro-D-Glucose

 

作者: T.J. Tewson,   M. Soderlind,  

 

期刊: Journal of Carbohydrate Chemistry  （Taylor Available online 1985）
卷期: Volume 4, issue 4  

页码: 529-543

 

ISSN:0732-8303

 

年代: 1985

 

DOI:10.1080/07328308508082675

 

出版商: Taylor & Francis Group

 

数据来源: Taylor

 

摘要:

1-Propenyl 4,6-Q-benzylidine-β-D-mannopyranoside-2,3-cyclic sulfate was prepared from methyl α-D-mannopyranoside. This compound reacts cleanly with tetramethylammonium fluoride, followed by add hydrolysis (2N HC1), to give 2-deoxy-2-fluoro-D-glucose. The reaction is suitable for use with the short lived radionuclide fluorlne-18 (t1/2,=110 minutes).

 

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