Calorimetry of High Polymers. I. Automatic Temperature Recording and Control of Adiabatic Jackets
作者:
Malcolm Dole,
W. P. Hettinger,
Norman Larson,
J. A. Wethington,
A. E. Worthington,
期刊:
Review of Scientific Instruments
(AIP Available online 1951)
卷期:
Volume 22,
issue 11
页码: 812-817
ISSN:0034-6748
年代: 1951
DOI:10.1063/1.1745769
出版商: AIP
数据来源: AIP
摘要:
This paper describes an adiabatic aneroid calorimeter for the measurement of the specific heat of high polymers over the temperature range −20 to 300°C.The temperature of its adiabatic jacket can be automatically recorded and, for the most part, automatically controlled, thus making possible the convenient study of temperature drifts, heat exchanges, and methods of correcting for such errors. Duplicate experiments have been carried out within an average deviation of 0.5 to 0.6 percent error, but the absolute error may be between one or two percent.
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