Practical aspects to the use of indirect fourier transformation methods
作者:
Karl Müller,
Otto Glatter,
期刊:
Die Makromolekulare Chemie
(WILEY Available online 1982)
卷期:
Volume 183,
issue 2
页码: 465-479
ISSN:0025-116X
年代: 1982
DOI:10.1002/macp.1982.021830216
出版商: Hüthig&Wepf Verlag
数据来源: WILEY
摘要:
AbstractPractical hints for the application of the indirect Fourier transformation method are given. In detail there are discussed the problems of stabilization of the least squares routine, the estimation of the maximum dimension of the particles, the choice of an appropriate number of the spline functions, the combination of scattering functions measured with different primary beam geometry, standard deviation and error propagation of the solution functions, influence of the interparticle interference effect and background scattering on the results, determination of the radius of gyration and the scattering intensity at zero angle and finally the possibility of simulation of measuring curves starting with model bodies is described. It is attempted to demonstrate the advantages of indirect Fourier transformation on hand of several practical examples.
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