An Open Vessel, Pulse-Microwave Technique for Wet Ashing of Metal-Contaminated Animal Tissues
作者:
P. Aysola,
P.D. Anderson,
C.H. Langford,
期刊:
Analytical Letters
(Taylor Available online 1988)
卷期:
Volume 21,
issue 11
页码: 2003-2010
ISSN:0003-2719
年代: 1988
DOI:10.1080/00032718808059886
出版商: Taylor & Francis Group
关键词: Wet ashing;fish;mammalian liver;metal assays;pulse microwave
数据来源: Taylor
摘要:
Wet ashing of whole fish arid standard mammalian liver samples for metal determinations is effectively achieved through low power pulse microwave treatment using a domestic grade microwave oven. The reaction is carried out in an open Erlenmeyer flask while held within a much larger sealed container. The latter may be any inexpensive vessel that is microwave proof. The power setting is approximately 70 watts. The oven is programmed to deliver microwaves for 10 seconds every three minutes for a total of 19 minutes. Efficiency of recovery is generally within 10% of the known amounts. The pulse microwave protocol avoids the high temperatures and pressures that create the risk of explosions.
点击下载:
PDF (213KB)
返 回