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Method for Observing and Controlling Microcracks in Ceramics

 

作者: Martin H. Leipold,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1970)
卷期: Volume 41, issue 6  

页码: 818-819

 

ISSN:0034-6748

 

年代: 1970

 

DOI:10.1063/1.1684655

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A technique has been developed by which a microcrack may be propagated in a controlled manner through a small slab, with simultaneous microscopic observation of the path of the crack and the force changes occurring during propagation. For studies of grain boundaries effects, specimens require grain sizes at least as large as specimen thickness (∼50 &mgr;) in order to define the effect of a single boundary on the crack path. Crack behavior may be observed by means of optical microscopy and would be suitable for scanning or transmission electron microscopy. Application of the technique to ceramic bicrystals indicates strong crack pinning points within the individual crystals as well as at the grain boundaries. In polycrystalline materials, these pinning points result in a start‐stop process which is repeated numerous times.

 

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