A simple NMR system was used for measurement of the o&sngbnd;H2concentration in the solid phase. It was found that the system must be calibrated, as the integral of the NMR absorption curve is not proportional to the o&sngbnd;H2concentration, which was suggested earlier. The influence of the quantum diffusion below 4 K and 0.35 o&sngbnd;H2content on the results is reported.