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Improved pressure calibration system using the rubyR1fluorescence

 

作者: Hubert E. King,   Charles T. Prewitt,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1980)
卷期: Volume 51, issue 8  

页码: 1037-1039

 

ISSN:0034-6748

 

年代: 1980

 

DOI:10.1063/1.1136375

 

出版商: AIP

 

数据来源: AIP

 

摘要:

When measuring pressures in the diamond anvil cell, undersirable line broadening and wavelength shifts result if small ruby crystals are used in a calibration system designed for large ones. These effects can be eliminated through the proper choice of objective lens, condensing lens, and slit system. Using such a system, we obtained excellent results with samples as small as 30 &mgr;m. In addition, we describe the use of the spectrum from a neon light to provide an internal wavelength standard during the measurement of the ruby spectrum. This eliminates the stripchart ‐ wavelength drive synchronization error, a potential source of large errors. A calculation of the estimated error associated with a typical pressure measurement indicates that, for small ruby samples, the pressure can be determined with a precision of ±0.5 kbar.

 

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