Improved pressure calibration system using the rubyR1fluorescence
作者:
Hubert E. King,
Charles T. Prewitt,
期刊:
Review of Scientific Instruments
(AIP Available online 1980)
卷期:
Volume 51,
issue 8
页码: 1037-1039
ISSN:0034-6748
年代: 1980
DOI:10.1063/1.1136375
出版商: AIP
数据来源: AIP
摘要:
When measuring pressures in the diamond anvil cell, undersirable line broadening and wavelength shifts result if small ruby crystals are used in a calibration system designed for large ones. These effects can be eliminated through the proper choice of objective lens, condensing lens, and slit system. Using such a system, we obtained excellent results with samples as small as 30 &mgr;m. In addition, we describe the use of the spectrum from a neon light to provide an internal wavelength standard during the measurement of the ruby spectrum. This eliminates the stripchart ‐ wavelength drive synchronization error, a potential source of large errors. A calculation of the estimated error associated with a typical pressure measurement indicates that, for small ruby samples, the pressure can be determined with a precision of ±0.5 kbar.
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