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Simultaneous Determination of Phenylbutazone, Flunixin, Indomethacin and 4 Methylaminoantipyrene with Novel use of an Ion-Pairing Step-Gradient HPLC Methodology

 

作者: L.G. Tillman,   G.E. Hardee,  

 

期刊: Analytical Letters  （Taylor Available online 1985）
卷期: Volume 18, issue 15  

页码: 1897-1904

 

ISSN:0003-2719

 

年代: 1985

 

DOI:10.1080/00032718508062915

 

出版商: Taylor & Francis Group

 

数据来源: Taylor

 

摘要:

An inexpensive step-gradient elution of the above nonsteroidal anti-inflammatory drugs (NSAIDs) using HPLC is described. The method involves: ion pairing the acid NSAIDs with tetrabutylammonium hydroxide (TBA) at pH 7.2, a stepwise change between two mobile phases differing only in solvent strength, and a “dilute and shoot” plasma sample preparation.

 

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