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ORGANIC DEUTERIUM COMPOUNDS: XIV. PREPARATION OF DEUTERATED METHYL BENZENES

 

作者: R. Renaud,   L. C. Leitch,  

 

期刊: Canadian Journal of Chemistry  （NRC Available online 1956）
卷期: Volume 34, issue 2  

页码: 98-102

 

ISSN:0008-4042

 

年代: 1956

 

DOI:10.1139/v56-011

 

出版商: NRC Research Press

 

数据来源: NRC

 

摘要:

The synthesis of toluene-α-d3,o-chlorotoluene-α-d3, andm-xylene-α,α′-d6from benzotrichloride,o-chlorobenzotrichloride, and α,α′ hexachloro-m-xylene respectively is reported using zinc and acetic acid-das the dechlorinating agent. The preparation of acetic acid-dof optimum isotopic purity is described.

 

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