A broadband nuclear magnetic resonance spectrometer: Digital phase shifting and flexible pulse programmer
作者:
Xiao Wu,
Donald A. Patterson,
Leslie G. Butler,
Joel B. Miller,
期刊:
Review of Scientific Instruments
(AIP Available online 1993)
卷期:
Volume 64,
issue 5
页码: 1235-1238
ISSN:0034-6748
年代: 1993
DOI:10.1063/1.1144122
出版商: AIP
数据来源: AIP
摘要:
A simple, low‐cost pulse nuclear magnetic resonance (NMR) spectrometer is described. There are two key features of the instrument: (1) all radio frequency phase shifting is done digitally with a new‐generation frequency synthesizer and (2) the pulse programmer is based on a high‐speed 32‐bit parallel interface card in a desktop computer. The spectrometer is well suited for single‐frequency channel experiments such as nuclear quadrupole resonance and deuterium quadrupole echo NMR experiments. Because the rf phase shifting is done digitally, the spectrometer operates easily over a wide frequency range, here 10–300 MHz. The pulse programmer and other software functions are written in LabView, a graphical programming language.
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