Background Reduction in IR Spectroscopy Using a Highly Scattering Filter
作者:
Mikio Kaihara,
Hiroaki Mametsuka,
Hideo Iwata,
Yohichi Gohshi,
期刊:
Analytical Letters
(Taylor Available online 1988)
卷期:
Volume 21,
issue 4
页码: 681-688
ISSN:0003-2719
年代: 1988
DOI:10.1080/00032718808081247
出版商: Taylor & Francis Group
关键词: FT-IR;background;baseline;transmission method;highly scattering filter
数据来源: Taylor
摘要:
There are many methods for measuring FT-IR spectra, for example, transmission, diffuse reflection, attenuated total reflection and so on. It is said that the transmission method is the most reliable method for qualitative and quantitative analysis of FT-IR spectra. The spectra of highly scattering samples such as coals or amorphous silicon powders measured by the transmission method, however, have large backgrounds with small relevant absorption peaks. Therefore, we investigated measuring methods for reducing the background itself. As a result, using a highly scattering 1R filter, we could clearly distinguish absorption peaks of amorphous silicon powders that were not found in IR spectrum measured by the normal transmission method. Our highly scattering filter is composed of fine Csl powders(<125*10−6m) and fine KBr powders(<125*10−6m).
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