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High‐performance cryogenic pulsed NMR spectrometer

 

作者: B. M. Wood,   R. F. Code,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1981)
卷期: Volume 52, issue 3  

页码: 386-390

 

ISSN:0034-6748

 

年代: 1981

 

DOI:10.1063/1.1136607

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A pulsed NMR spectrometer for cryogenic use is described. It includes an improved coupling scheme which is suitable for installation in most cryostats. An rf preamplifier has been developed which offers wide bandwidth, high gain, low noise and fast recovery (⩽2 &mgr;s). While the spectrometer was designed for a resonance frequency of 27 MHz, extension from 4–100 MHz is discussed. At 27 MHz the bandwidth of the free‐induction decay is 1 MHz, and the dead time, after the end of the rf pulse, is 3.6 ms. Techniques are presented for reducing the dead time, the noise, and the amplitude of ground loops as well as extending the signal bandwidth and dynamic range.

 

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