Magnetically Suspended Equilibrium Ultracentrifuge
作者:
J. W. Beams,
R. D. Boyle,
P. E. Hexner,
期刊:
Review of Scientific Instruments
(AIP Available online 1961)
卷期:
Volume 32,
issue 6
页码: 645-650
ISSN:0034-6748
年代: 1961
DOI:10.1063/1.1717460
出版商: AIP
数据来源: AIP
摘要:
An improved magnetically supported equilibrium ultracentrifuge is described for the determination of molecular weights and molecular weight averages. The rotor is magnetically suspended in a vacuum. The rotor is driven to operating speed by an electric motor or by an air turbine. The rotor is allowed to ``coast'' freely during the course of the sedimentation and loses about 1 rps per day. An improved Jamin interferometer is used to measure the concentration in the ultracentrifuge cell both before and after equilibrium has been established. A precision of the order of 0.1% is obtained for monodisperse substances over a very wide molecular weight range.
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