A Rapid Method for Preparing Powder Camera Specimens with Cellulose Acetate Capillary Tubes
作者:
Karl E. Beu,
Howard H. Claassen,
期刊:
Review of Scientific Instruments
(AIP Available online 1948)
卷期:
Volume 19,
issue 3
页码: 179-180
ISSN:0034-6748
年代: 1948
DOI:10.1063/1.1741227
出版商: AIP
数据来源: AIP
摘要:
Several details are described in the preparation of capillary tubes for x‐ray power specimens which greatly facilitate the synthesis of such tubes and their subsequent removal from the pilot wire. The over‐all method employed is essentially that of Frickeet al.Wires of 22‐gauge copper, after annealing in an atmosphere of helium, are cleaned and dipped into the cellulose acetate solution by means of a crank‐driven rack. The rate of withdrawal determines the wall thickness. A method is given for centering the filled specimen tubes precisely in the powder camera by the use of a centering jig.
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