Photochehical Fluorimetric Determination of Primaquine in a Flowing Solvent with Application to Blood Serum
作者:
M. Tsuchiya,
E. Torres,
J.J. Aaron,
J.D. Winefordner,
期刊:
Analytical Letters
(Taylor Available online 1984)
卷期:
Volume 17,
issue 16
页码: 1831-1841
ISSN:0003-2719
年代: 1984
DOI:10.1080/00032718408077186
出版商: Taylor & Francis Group
关键词: Fluorescence;photochemical conversion;blood serum;primaquine.
数据来源: Taylor
摘要:
Primaquine in a flowing solvent is photolyzed with a 200 W Xe-Hg arc lamp and the intensely fluorescent photochemical product is measured in a fluorimeter. The effect of solvent composition and pH, irradiation time, and excitation conditions are evaluated. Primaquine in blood serum is measured by introducing a sample of blood serum into the flowing stream and performing the photochemical-fluorescence measurement. The fluorescence background of blood serum was very low allowing a detection limit of less than 0.1 μg/mL. Excellent recoveries were obtained.
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