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The processing of diffraction data taken on a screenless Weissenberg camera for macromolecular crystallography

 

作者: T. Higashi,  

 

期刊: Journal of Applied Crystallography  (WILEY Available online 1989)
卷期: Volume 22, issue 1  

页码: 9-18

 

ISSN:1600-5767

 

年代: 1989

 

DOI:10.1107/S0021889888009562

 

出版商: International Union of Crystallography

 

数据来源: WILEY

 

摘要:

A method has been developed based on Rossmann's [J. Appl Cryst.(1979).12, 225–238] treatment of oscillation camera data for processing of X‐ray diffraction data collected on a screenless Weissenberg camera for macromolecular crystals [Sakabe (1983).J. Appl. Cryst.16, 542–547]. Crystal orientation parameters and film orientation parameters are refined by minimizing the discrepancies between the calculated and observed positions of reflections on a film. A data processing example is presented. Intensities were collected using a synchrotron radiation source and the imaging plate as a detector. The results show that the quality of the data is good, as judged by the agreement of the equivalent reflections. An absorption correction based on the use of the empirical Fourier expansion method reduced theRvalue and improved the correlations between Bijvoet differences observed on the different imaging plate expo

 

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