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Investigation of Instrument Parameters for the Application of Peroxyoxalate Cheminescence Detection to Microbore Chromatography

 

作者: MaryLynn Grayeski,   AndrewJ. Weber,  

 

期刊: Analytical Letters  （Taylor Available online 1984）
卷期: Volume 17, issue 13  

页码: 1539-1552

 

ISSN:0003-2719

 

年代: 1984

 

DOI:10.1080/00032718408065328

 

出版商: Taylor & Francis Group

 

关键词: Peroxyoxalate chemiluminscence;microbore HPLC

 

数据来源: Taylor

 

摘要:

Peroxyoxalate chemiluminescence generated by the reaction of an oxalate and hydrogen peroxide in the presence of a fluorophor was evaluated as a detection system for microbore liquid chromatography. The results of studies on instrumental parameters show that the signal is increased with short reaction lines, increasing flow cell volume, and enhanced response through detectors with improved optics.

 

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