The droplet size distribution (DSD) of unstable water/oil dispersions has been studied with a new technique. The technique is based on a fast dilution of the dispersion injected into an analysis vessel where the DSD is analyzed with a video camera and a image analyzing tool. Dispersions generated with no pressure drop in the flow rig were compared to those generated with a pressure drop over a needle valve. The latter dispersion showed a much narrower DSD and a lower average droplet diameter. The results are from preliminary experiments in order to evaluate the method.