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Analysis of standard reference materials following digestion using a modified appliance grade microwave oven

 

作者: John C. Schaumloffel,   William F. Siems,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1996)
卷期: Volume 67, issue 12  

页码: 4321-4323

 

ISSN:0034-6748

 

年代: 1996

 

DOI:10.1063/1.1147533

 

出版商: AIP

 

数据来源: AIP

 

摘要:

Microwave digestion provides a rapid means of sample preparation in the analytical laboratory. The major disadvantage of this method is the high cost of commercial microwave digestion systems. Modifications to the magnetron timing circuits of an appliance grade oven to make it suitable for sealed vessel microwave digestion are reported. The oven was modified without alteration to the irradiation cavity, and all initial safety features remain intact. Following digestion with the modified oven, NIST Standard Reference Materials (SRMs) were analyzed by inductively coupled plasma emission spectroscopy. The analytical data are similar to the certified concentrations in the SRMs, indicating that the modified oven provides a durable, rapid, cost‐effective means of sample preparation. ©1996 American Institute of Physics.

 

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