Analysis of standard reference materials following digestion using a modified appliance grade microwave oven
作者:
John C. Schaumloffel,
William F. Siems,
期刊:
Review of Scientific Instruments
(AIP Available online 1996)
卷期:
Volume 67,
issue 12
页码: 4321-4323
ISSN:0034-6748
年代: 1996
DOI:10.1063/1.1147533
出版商: AIP
数据来源: AIP
摘要:
Microwave digestion provides a rapid means of sample preparation in the analytical laboratory. The major disadvantage of this method is the high cost of commercial microwave digestion systems. Modifications to the magnetron timing circuits of an appliance grade oven to make it suitable for sealed vessel microwave digestion are reported. The oven was modified without alteration to the irradiation cavity, and all initial safety features remain intact. Following digestion with the modified oven, NIST Standard Reference Materials (SRMs) were analyzed by inductively coupled plasma emission spectroscopy. The analytical data are similar to the certified concentrations in the SRMs, indicating that the modified oven provides a durable, rapid, cost‐effective means of sample preparation. ©1996 American Institute of Physics.
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