A high-pressure cell for optical microscopy and measurements on the phase diagram of poly(diethylsiloxane)
作者:
T. Reck,
E. Sautter,
W. Dollhopf,
W. Pechhold,
期刊:
Review of Scientific Instruments
(AIP Available online 1998)
卷期:
Volume 69,
issue 4
页码: 1823-1827
ISSN:0034-6748
年代: 1998
DOI:10.1063/1.1148848
出版商: AIP
数据来源: AIP
摘要:
A new high-pressure cell as useful equipment for a polarizing microscope is described. Measurements in a temperature range between−40and+270 °Cunder hydrostatic pressures up to 300 MPa allow for example the observation of polymer morphology and phase transitions. In addition to a documentation on video and photograph, respectively, the computer-controlled light intensity measurement offers the possibility of a quantitative analysis. Investigations on the phase diagram of poly(diethylsiloxane) have been carried out and show, that the transition temperature from mesophase to isotropic melt decreases with increasing pressure for pressures above 160 MPa. ©1998 American Institute of Physics.
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