Use of Micelles in the TLC Separation of Polynuclear Aromatic Compounds and Amino Acids
作者:
DanielW. Armstrong,
Marguerite McNeely,
期刊:
Analytical Letters
(Taylor Available online 1979)
卷期:
Volume 12,
issue 12
页码: 1285-1291
ISSN:0003-2719
年代: 1979
DOI:10.1080/00032717908067919
出版商: Taylor & Francis Group
关键词: Micellar Chromatography;Normal and Reversed Micelles;PNA;Amino Acids.
数据来源: Taylor
摘要:
The polynuclear aromatic compounds (PNA): anthracene, napthalene, phenanthrene, pyrene, pyrenecarboxaldehyde, benzo (a) pyrene, benzo (e) pyrene, perylene and fluorene can be chromatographed on polyamide TLC sheets using an aqueous micellar solution cf sodium dodecylsulfate (SDS) as the mobile phase. Reversed micellar solutions (of sodium dioctylsulfosuccinate) were used in a reverse phase chromatographic separation of amino acids. Some amino acids tended to streak slightly rather than move as discrete spots. Conditions could be adjusted, however, so that most of the amino acids and all PNA's would move as spots.
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