Variable‐temperature solid‐state nuclear‐magnetic‐resonance probe for superconducting magnets operating in the range 3–350 K
作者:
Keith Carduner,
Marco Villa,
David White,
期刊:
Review of Scientific Instruments
(AIP Available online 1984)
卷期:
Volume 55,
issue 1
页码: 68-74
ISSN:0034-6748
年代: 1984
DOI:10.1063/1.1137592
出版商: AIP
数据来源: AIP
摘要:
A versatile, variable‐temperature (3–350 K continuous), vacuum cold‐finger, solid‐state nuclear‐magnetic‐resonance (NMR) probe is described and its characteristics in several applications are discussed. The single‐coil probe is specifically designed for use in superconducting magnets with bores as small as 2.5 in. and is suitable for both single‐ and double‐resonance experiments. The tuning arrangement allows for multinuclear data acquisition without the necessity of breaking the vacuum. Various adaptations to the cold finger suitable for a variety of different solids, e.g., powders, amorphous materials (glasses), condensables, and single crystals are presented including a single‐axis goniometer operable over the entire temperature range.
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