Disaccommodation and ferromagnetic resonance measurements for single crystal titanium‐doped lithium ferrites are presented. Magnetic disaccommodation is performed at 1 kHz from 77 to 400 K while ferromagnetic resonance is carried out at 11 GHz from 77 to 300 K. Ferromagnetic resonance line shape asymmetry and anisotropy field data are also shown. A relationship between the asymmetry and the disaccommodation spectra is suggested. ©1995 American Institute of Physics.