1H and31P NMR spectra of the phenyl ester of dichlorophosphoric acid in a nematic phase
作者:
J. Hansen,
J. P. Jacobsen,
期刊:
Organic Magnetic Resonance
(WILEY Available online 1981)
卷期:
Volume 15,
issue 1
页码: 29-32
ISSN:0030-4921
年代: 1981
DOI:10.1002/mrc.1270150108
出版商: John Wiley&Sons Limited
数据来源: WILEY
摘要:
AbstractThe1H and31P NMR spectra of the phenyl ester of dichlorophosphoric acid dissolved in Merck nematic phase IV have been recorded and analysed. The values of the dipole dipole couplings have been discussed in terms of several different geometric models. Non‐planarity of C‐1, O, P and the phenyl ring must be assumed in order to account for the results; a twist angle of 49° was f
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