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A heatable large volume high pressure cell for neutron powder diffraction: The Kiel-Berlin Cell I

 

作者: K. Knorr,   K. Fu¨tterer,   B. Annigho¨fer,   W. Depmeier,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1997)
卷期: Volume 68, issue 10  

页码: 3817-3822

 

ISSN:0034-6748

 

年代: 1997

 

DOI:10.1063/1.1148033

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A heatable high pressure cell for angle dispersive neutron powder diffraction has been developed. This cell, called Kiel-Berlin Cell I, is of the piston–cylinder-type and based on a design first introduced by McWhan. High temperature conditions under high pressure are achieved by a graphite resistance heater surrounding the sample container. The cell operates up to temperatures of 700 K and pressures of 1.5 GPa, simultaneously. We report the design of the cell along with calibration data. We also give a brief and representative account of pressure-temperature-dependent studies in which the present cell was used. ©1997 American Institute of Physics.

 

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