Morphology definition by disclinations and dislocations in a mesostructured silicate crystal
作者:
J. Feng,
Q. Huo,
P. M. Petroff,
G. D. Stucky,
期刊:
Applied Physics Letters
(AIP Available online 1997)
卷期:
Volume 71,
issue 5
页码: 620-622
ISSN:0003-6951
年代: 1997
DOI:10.1063/1.119810
出版商: AIP
数据来源: AIP
摘要:
Curved surface morphologies resulting from disclinations are unusual in inorganic phases because the relatively large lattice energies generally permit only translational dislocations. In this letter, we show, however, that disclinations can be readily observed and identified in composite organic/inorganic phases. Disclinations and dislocations in MCM-41, a two-dimensional hexagonal (p6mm) mesophase crystal synthesized using silicate and surfactant precursors, were investigated by using transmission electron microscopy. We observed two types of dislocations and two types of disclinations. All dislocations observed are of the smallest Burgers vectora(the basis vector). Dislocation dipoles and disclination quadrupoles appear more frequently than isolated ones. ©1997 American Institute of Physics.
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