Single-chain single crystals of gutta-percha
作者:
Lizhi Liu,
Fengyu Su,
Hongshuang Zhu,
Hong Li,
Enle Zhou,
Ruifang Yan,
Renyuan Qian,
期刊:
Journal of Macromolecular Science, Part B
(Taylor Available online 1997)
卷期:
Volume 36,
issue 2
页码: 195-203
ISSN:0022-2348
年代: 1997
DOI:10.1080/00222349708220425
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
Single-chain single crystals of gutta-percha have been observed by transmission electron microscopy of atomizer-sprayed particles deposited from a very dilute solution in chloroform onto a carbon film which had a filter paper wetted with ethanol in contact with its under side. Selected-area electron diffraction patterns of crystals having no definite crystal profiles showed that the crystals were of the low-melting crystalline form and that the chain segments in the single crystals were standing up from the substrate during crystallization. In cases of single crystals showing sharply defined crystal profiles, electron diffraction patterns showed that they were neither of the low-melting form nor the high-melting form. The structure of this new crystalline modification needs further studies.
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