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1. |
Construction and application of a cold on‐column injection system for capillary gas chromatography |
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Journal of High Resolution Chromatography,
Volume 8,
Issue 2,
1985,
Page 62-68
R. F. Arrendale,
O. T. Chortyk,
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摘要:
AbstractA cold on‐column injection system for capillary gas chromatography (GC) applications was constructed. It was based upon a conventional split/splitless capillary GC inlet, which in turn was a modification of a conventional packed GC column inlet. The heart of the laboratory constructed cold on‐column inlet design was a disposable pyrex micro‐sampling pipet, which functioned as a needle guide for sample injection. The sample was injected through a traditional GC septum. Construction of the injection system is described and applications are illustrated by separations of a variety of complex mix
ISSN:0935-6304
DOI:10.1002/jhrc.1240080202
出版商:Wiley Subscription Services, Inc., A Wiley Company
年代:1985
数据来源: WILEY
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2. |
Determination of metabolites relating to the tryptophan‐NAD pathway in rat urine by cellulose high performance thin‐layer chromatography |
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Journal of High Resolution Chromatography,
Volume 8,
Issue 2,
1985,
Page 69-72
M. Yamada,
Y. Minami,
S. Yuyama,
T. Suzuki,
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摘要:
AbstractHigh performance thin‐layer chromatography (HPTLC) was used to determine 12 metabolites of the tryptophan‐NAD pathway in rat urine. The method of separation described in the previous report was improved. The metabolites were separated on the cellulose plate by using five multiple developments with four solvent systems. The plate was scanned by the TLC scanner at 254 nm and the amounts of the metabolites were calculated by comparing peak areas of the scanning curves obtained for the urine sample and for the authentic standards. This procedure can be used as a semiquantitative determination method for the metabolites in biological flu
ISSN:0935-6304
DOI:10.1002/jhrc.1240080203
出版商:Wiley Subscription Services, Inc., A Wiley Company
年代:1985
数据来源: WILEY
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3. |
Sequential centrifugal layer chromatography (SCLC): A New technique for the isolation of natural compounds. Part 1: Description of the method and practical aspects |
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Journal of High Resolution Chromatography,
Volume 8,
Issue 2,
1985,
Page 73-76
Sz. Nyiredy,
C. A. J. Erdelmeier,
O. Sticher,
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PDF (304KB)
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摘要:
AbstractSequential centrifugal layer chromatography (SCLC), a new preparative planar separation technique, combines the advantages of preparative centrifugal layer chromatography (CLC) and analytical, horizontal, anticircular, and sequential thin‐layer chromatography (TLC). In this on‐line preparative method, solvent delivery is locally and temporally variable, which means that the mobile phase can be brought onto the plate at any desired place.The SCLC apparatus operates in two modes: circular, with the help of centrifugal force in an inclined position, and anticircular, by means of capillary action in a horizontal position. These two operation modes can be combined and repeated as often as required, hence the separation space becomes practically unlimited. In this way the capacity and separation performance is significantly increased.In the present paper the apparatus and the method are described and some practical aspects are mentio
ISSN:0935-6304
DOI:10.1002/jhrc.1240080204
出版商:Wiley Subscription Services, Inc., A Wiley Company
年代:1985
数据来源: WILEY
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4. |
A means of improving the performance of heat‐shrinkable, polytetrafluoroethylene joints in capillary gas liquid chromatography |
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Journal of High Resolution Chromatography,
Volume 8,
Issue 2,
1985,
Page 77-78
V. Pretorius,
P. J. Apps,
E. R. Rohwer,
K. H. Lawson,
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ISSN:0935-6304
DOI:10.1002/jhrc.1240080205
出版商:Wiley Subscription Services, Inc., A Wiley Company
年代:1985
数据来源: WILEY
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5. |
Study of salt in gel filtration of proteins on TSKgel G3000SW |
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Journal of High Resolution Chromatography,
Volume 8,
Issue 2,
1985,
Page 78-79
Y. Kato,
T. Hashimoto,
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PDF (139KB)
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ISSN:0935-6304
DOI:10.1002/jhrc.1240080206
出版商:Wiley Subscription Services, Inc., A Wiley Company
年代:1985
数据来源: WILEY
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6. |
Unusual selectivity of trifluoropropyl silicone capillary column |
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Journal of High Resolution Chromatography,
Volume 8,
Issue 2,
1985,
Page 80-81
G. J. McManemin,
W. Reuter,
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ISSN:0935-6304
DOI:10.1002/jhrc.1240080207
出版商:Wiley Subscription Services, Inc., A Wiley Company
年代:1985
数据来源: WILEY
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7. |
Analysis of nitro‐4H‐cyclopenta[def]phenanthrenes in ambient air by fused silica capillary gas chromatography/mass spectrometry |
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Journal of High Resolution Chromatography,
Volume 8,
Issue 2,
1985,
Page 82-84
Th. Ramdahl,
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ISSN:0935-6304
DOI:10.1002/jhrc.1240080208
出版商:Wiley Subscription Services, Inc., A Wiley Company
年代:1985
数据来源: WILEY
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8. |
Versatile injection device for injecting 0.5‐100 μl for capillary gas chromatography |
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Journal of High Resolution Chromatography,
Volume 8,
Issue 2,
1985,
Page 85-87
F. Etzweiler,
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PDF (254KB)
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ISSN:0935-6304
DOI:10.1002/jhrc.1240080209
出版商:Wiley Subscription Services, Inc., A Wiley Company
年代:1985
数据来源: WILEY
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9. |
High performance liquid chromatographic method for 2,3‐dinor‐6‐keto‐prostaglandin F1α |
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Journal of High Resolution Chromatography,
Volume 8,
Issue 2,
1985,
Page 88-89
J. Casas,
J. Roselló,
E. Gelpí,
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ISSN:0935-6304
DOI:10.1002/jhrc.1240080210
出版商:Wiley Subscription Services, Inc., A Wiley Company
年代:1985
数据来源: WILEY
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10. |
Separation of twelve monomethylbenz[a]anthracenes on the liquid crystal and isotropic stationary phases in relation to the shape of their molecules |
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Journal of High Resolution Chromatography,
Volume 8,
Issue 2,
1985,
Page 90-92
H. Lamparczyk,
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PDF (256KB)
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ISSN:0935-6304
DOI:10.1002/jhrc.1240080211
出版商:Wiley Subscription Services, Inc., A Wiley Company
年代:1985
数据来源: WILEY
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