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11. |
High Performance Liquid Chromatographic Assay of Methoclopramide in Plasma Using a Silica Gel Column and An Aqueous Meobile Phase |
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Analytical Letters,
Volume 20,
Issue 1,
1987,
Page 131-140
RobertJ.Y. Shi,
WinniaL. Gee,
RogerL. Williams,
EmitT. Lin,
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摘要:
A high performance liquid chromatographic method for quantitating matoclopramide in plasma is presented. Proteins ara precipitated from the plasma sample with acetonitri la containing the internal standard, procainamida. The treated samples ara than analyzad using an Ultrasphere Si column, an aqueous solution at pH 7 of 65% CH3CN and 5.0 mM (NH4)2HPO4as a mobile phase, and a fluorescence detector. The retention times for drug and intarna1 standard ara 11.2 and 13.2 min, respectively. The caibration curve is Linear from 0.89 to 44.5 ng/ml. The detection limit is 0.89 ng/ml [signaL/hoisa = 31] for 0.2 ml plasma samples Pracision is measured by intraday and intarday coefficients o f variation, which are less than 10%. This method is currently being used for pharmacokinetic studies of methoclopramide.
ISSN:0003-2719
DOI:10.1080/00032718708082241
出版商:Taylor & Francis Group
年代:1987
数据来源: Taylor
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12. |
Determination of Penicillins in pure form and in Pharmaceuticals |
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Analytical Letters,
Volume 20,
Issue 1,
1987,
Page 141-159
Basilio Morelli,
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摘要:
A rapid and convenient method is described for the determination of thirteen commercially available penicillins: methicillin Na, oxacillin Na, cloxacillin Na, dicloxacillin Na, nafcillin Na, ampicillin Na, amoxicillin, carbenicillin Na, penicillin-G Na, penicillin-G procain salt, penicillin-G benzathine salt, phenoxymethylpenicillinic acid K and phenoxymethylpenicillinic acid benzyl ester sulphoxide.
ISSN:0003-2719
DOI:10.1080/00032718708082242
出版商:Taylor & Francis Group
年代:1987
数据来源: Taylor
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13. |
Comments: A Comments to the Papers “Spectrophotometric Determantion of Hydroxylamine, Glycine, Methionine by Using Sodium Ntiroprusside as a Complexing Agents” and “Spectrophotometric Determanation Ofthiosulfate Thiocyanate and Thiourea Ions by Using Sodium Nitroprusside as a Complexing Agents” |
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Analytical Letters,
Volume 20,
Issue 1,
1987,
Page 161-167
Ágnes Kathó,
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摘要:
The use of nitroprusside ion, as a reagent for detection of a varicty of inorganic and organic compounds has very long history1.
ISSN:0003-2719
DOI:10.1080/00032718708082243
出版商:Taylor & Francis Group
年代:1987
数据来源: Taylor
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14. |
Editorial board page for “Analytical Letters”, Volume 20, Number 1 |
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Analytical Letters,
Volume 20,
Issue 1,
1987,
Page -
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PDF (100KB)
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摘要:
This is a scanned image of the original Editorial Board page(s) for this issue.
ISSN:0003-2719
DOI:10.1080/00032718708082230
出版商:Taylor & Francis Group
年代:1987
数据来源: Taylor
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