Contribution to the knowledge of metanethole IV
作者:
J. M. V. D. Zanden,
G. de Vries,
期刊:
Recueil des Travaux Chimiques des Pays‐Bas
(WILEY Available online 1955)
卷期:
Volume 74,
issue 1
页码: 52-58
ISSN:0165-0513
年代: 1955
DOI:10.1002/recl.19550740107
出版商: WILEY‐VCH Verlag
数据来源: WILEY
摘要:
AbstractThe structure of some of the compounds mentioned in our investigation of metanethole was still under discussion.It has been found that metanethole has the structure V. When 1‐p‐methoxyphenyl‐2‐methyl‐3‐ethyl‐6‐methoxyindene‐1, formula I, is brominated2), the product IV is obtained. To the metanethole oxidation product, m.p. 115‐116°3), formula X4)5) applies. With hydrazine hydrate it gives XI. Afterwards we also found this substance mentioned in work byA. Müller5A).The following substances not mentioned in the literature have now been synthesized by us: β‐p‐methoxyphenyl‐β‐m‐methoxyphenylcinnamic acid, m.p. 154‐155°, formula VII, β‐p‐methoxyphenyl‐β‐m‐methoxyphenyl‐β‐hydr
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