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Studies on the syntheses of heteroeyelie compounds. Part DVI. Synthesis of oxynilidine and nitidine

 

作者: Tetsuji Kametani,   Kazuo Kigasawa,   Mineharu Hiiragi,   Osamu Kusama,  

 

期刊: Journal of Heterocyclic Chemistry  （WILEY Available online 1973）
卷期: Volume 10, issue 1  

页码: 31-33

 

ISSN:0022-152X

 

年代: 1973

 

DOI:10.1002/jhet.5570100107

 

出版商: Wiley‐Blackwell

 

数据来源: WILEY

 

摘要:

AbstractA benzyne type reaction of 1‐bromo‐3,4‐dimethoxybenzene (V) with 3,4‐dihydro‐6,7‐methylenedioxy‐I(2H)naphthalenone (VI) gave the tetralone derivative VII, which was converted into the amine IXviathe oxime VIII. A Mannich reaction of IX afforded the benzo[c]phen‐anthridine II which was then transformed into oxynitidine (I) an

 

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