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LCEC Detector with Graphite-Teflon Electode

 

作者: M.H. Shah,   I.L. Honigberg,  

 

期刊: Analytical Letters  (Taylor Available online 1983)
卷期: Volume 16, issue 15  

页码: 1149-1163

 

ISSN:0003-2719

 

年代: 1983

 

DOI:10.1080/00032718308077152

 

出版商: Taylor & Francis Group

 

关键词: Voltammetry;liquid chromatography;electrochemical detection;graphite-Teflon electrode;flow-cell;passivation

 

数据来源: Taylor

 

摘要:

A compression molded graphite-Teflon electrode is evaluated as a detector for the electrochemical detection of phenolic compounds, separated by reverse-phase high-performance liquid chromatography. Detection limits for these phenolic compounds range from 0.5–1 ng. Repetitive injections yield peak heights with RSDs less than 1%. Passivation of electrode surface by phenols is discussed. In addition, construction of a flow cell to be used in conjunction with graphite-Teflon electrode is also described.

 

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