LCEC Detector with Graphite-Teflon Electode
作者:
M.H. Shah,
I.L. Honigberg,
期刊:
Analytical Letters
(Taylor Available online 1983)
卷期:
Volume 16,
issue 15
页码: 1149-1163
ISSN:0003-2719
年代: 1983
DOI:10.1080/00032718308077152
出版商: Taylor & Francis Group
关键词: Voltammetry;liquid chromatography;electrochemical detection;graphite-Teflon electrode;flow-cell;passivation
数据来源: Taylor
摘要:
A compression molded graphite-Teflon electrode is evaluated as a detector for the electrochemical detection of phenolic compounds, separated by reverse-phase high-performance liquid chromatography. Detection limits for these phenolic compounds range from 0.5–1 ng. Repetitive injections yield peak heights with RSDs less than 1%. Passivation of electrode surface by phenols is discussed. In addition, construction of a flow cell to be used in conjunction with graphite-Teflon electrode is also described.
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