Mica Track Microfilters (MTM) are successful applied to separate two different and strongly mixed liquid phases (emulsion). The organic and the inorganic phase of the emulsion were 30% tributyl phosphate (TBP) in kerosene and 2 N HNO3(or H2O), respectively. Mica filters with sharp edges (i.e. etched with H2F2) and having pore sizes k of 8 μm > k > 2 μm are used to get under some well defined conditions a rather complete extraction of the aqueous phase out of the emulsion. The system was calibrated with the pure phases (water as well as TBP in kerosene), and the liquid throughput is shown as a function of the pore size of the filter. The throughput depends mainly on the pore size and not that much on the kind of liquid, it is slightly larger for water as compared to that of TBP in kerosene.