Neutron and Synchrotron Radiation High Pressure Experiments on Aluminate Sodalite Sr8[Al12O24](CrO4)2
作者:
R. Melzer,
W. Depmeier,
T. Vogt,
E. Gering,
期刊:
Crystal Research and Technology
(WILEY Available online 1995)
卷期:
Volume 30,
issue 6
页码: 767-773
ISSN:0232-1300
年代: 1995
DOI:10.1002/crat.2170300608
出版商: WILEY‐VCH Verlag
数据来源: WILEY
摘要:
AbstractHigh pressure powder diffraction experiments were carried out on the aluminate sodalite Sr8[Al12O24] · (CrO4)2using a miniature clamped cell with neutron radiation at the ILL and a diamond anvil cell with synchrotron radiation at Hasylab/Desy. The results of both experiments agree well. Lattice parameters were determined up to a pressure of 7.2 GPa. The average linear compressibility amounts to 4.3 · 10−3GPa−1, which corresponds to a linear bulk modulus of 233 GPa. The observation of superstructure reflections could be related to two new phase transitions. The first one occurs between 0.37 and 0.5 GPa, the second one at about 2.0 GPa. A final measurement at ambient pressure revealed the reversible character of the pressure induced phase transi
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