Thermomechanical Behavior of an Aromatic Polysulfone
作者:
JohnK. Gillham,
GeorgeF. Pezdirtz,
Lionel Epps,
期刊:
Journal of Macromolecular Science: Part A - Chemistry
(Taylor Available online 1969)
卷期:
Volume 3,
issue 6
页码: 1183-1195
ISSN:0022-233X
年代: 1969
DOI:10.1080/10601326908051944
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
The thermomechanical behavior (less than 1 Hz) of a newly available, high temperature, aromatic polysulfone has been investigated by the technique of lorsional braid analysis (TBA). Speculations concerning the synthesis and structure are discussed in terms of NMR and infrared spectroscopy, elemental analysis, and a review of the general literature on polysulfones. In addition to the glass transition at 287°C, a secondary relaxation was detected in the glassy state at −100°C by a mechanical loss maximum and change in modulus. The stability of the polysulfone at elevated temperatures in air and nitrogen as monitored by TBA, DTA, and TGA is reported. The influence of heat to 500°C, high doses of ionizing radiation, and water on the transitions of the polymer is discussed.
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