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Application of Electrochemical Detection for the Quantitation of 1, 4-Dihydroxy-5, 8-Bis-[2-(2-Hydroxyethyl) Aminoethylamino]-9,10-Anthracenedione Following Liquid Chromatography

 

作者: StevenT. Houpt,   RichardP. Baldwin,  

 

期刊: Analytical Letters  （Taylor Available online 1983）
卷期: Volume 16, issue 16  

页码: 1343-1354

 

ISSN:0003-2719

 

年代: 1983

 

DOI:10.1080/00032718308065248

 

出版商: Taylor & Francis Group

 

关键词: 1, 4-dihydroxy-5;8-bis[2-(2- hydroxyethy1) aminoethylamino]-9;10-anthracenedione;liquid chromatography with electrochemical detection

 

数据来源: Taylor

 

摘要:

Electrochemical monitoring of 1, 4-dihydroxy-5, 8-bis-[2-(2-hydroxyethy1) aminoethy amino]-9, 10-anthracenedione was employed for the quantitation of this cancer chemotherapy drug following high performance liquid chromatography. Detection was performed by oxidation of the compound at a glassy carbon electrode at +0.80 V vs. SCE. A rapid and convenient sample treatment procedure was developed which is suitable for determination involving physiological samples. A detection limit of 2 ng injected was obtained for urine samples.

 

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