Crystal and molecular structure of 8,8‐dimethyl‐8‐azoniabicyclo [5.1.0] octane iodide
作者:
L. M. Trefonas,
Robert Towns,
期刊:
Journal of Heterocyclic Chemistry
(WILEY Available online 1964)
卷期:
Volume 1,
issue 1
页码: 19-22
ISSN:0022-152X
年代: 1964
DOI:10.1002/jhet.5570010104
出版商: Wiley‐Blackwell
数据来源: WILEY
摘要:
AbstractThe crystal and molecular structure of 8, 8‐dimethyl‐8‐azoniabicyclo[5.1. 0]octane iodide has been elucidated. The aziridine ring is bridgedcisto the cycloheptane ring. The cycloheptane ring has been shown to have a distorted chair conformation. No close trans‐annular hydrogen distances have been observed. The compound crystallizes in the space group Pna21with unit cell dimensions a = 17.31, b= 8.58 and c=7.56Å. The final value of R=Σ ‖ Fo| ‐ | Fc‖/Σ| Fo| is 0.145 for the 734 obse
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