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Solid-Phase Extraction as a Clean-Up Procedure for the Liquid Chromatographic Determination of Benzoic and Sorbic Acids in Fruit-Derived Products

 

作者: B. Mandrou,   V. Nolleau,   E. Gastaldi,   H. Fabre,  

 

期刊: Journal of Liquid Chromatography & Related Technologies  (Taylor Available online 1998)
卷期: Volume 21, issue 6  

页码: 829-842

 

ISSN:1082-6076

 

年代: 1998

 

DOI:10.1080/10826079808000512

 

出版商: Taylor & Francis Group

 

数据来源: Taylor

 

摘要:

A liquid-chromatographic procedure is proposed for the simultaneous determination of benzoic and sorbic acids in fruit-derived products. Prior to the chromatographic separation, a clean-up pre-treatment of the sample is carried out off-line, using successively an anionic resin and a C18stationary phase as sorbent beds. After elution from the cartridges, the acids are separated and quantitated by LC with UV-absorbance detection. The validation tests show that the technique can be applied to different types of fruit-derived products (i.e. jams, dried fruits and almond paste).

 

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